Effect of moisture content and frequency variation on dielectric properties of bamboo (Phyllostachys heterocycla cv. pubescens)
Forest Industry
EFFECT OF MOISTURE CONTENT AND FREQUENCY VARIATION
ON DIELECTRIC PROPERTIES OF BAMBOO
(Phyllostachys heterocycla cv. pubescens)
Nguyen Thi Huong Giang1, Tran Van Chu2
1,2Vietnam National University of Forestry
SUMMARY
Moisture content of bamboo and frequency are the most important factors that affects dielectric properties of
bamboo material. Dielectric properties of bamboo is one of the most important factors to determine the high-
frequency hot pressing process parameters of glued laminated bamboo... Therefore, study on dielectric
properties of bamboo has important significance. Bamboo was adjusted moisture content under laboratory
conditions for 0-18%. Effect of moisture content and frequency variation on dielectric properties of bamboo
was determined by using the 4294A Precision Impedance Analyzer with the 16451B. Dielectric properties
including dielectric constant (e’) and dielectric loss tangent (tan d) have been done in the moisture content
range from 0% to 18% and in the frequency range from 60 Hz to 6 MHz. The results showed that the dielectric
constant (e’) and tan d increase with the increasing moisture content and decrease with the increasing
frequency. Dielectric constant and tan d increased slowly with the moisture content below fiber saturation point
(FSP), increased sharply with the moisture content around the FSP. Dielectric constant and tan d decreased
obviously with the frequency below 6 kHz, but changed slowly when it above 6 kHz.
Keywords: Bamboo, dielectric constant, dielectric loss tangent, frequency, moisture content.
Electric properties of both wood and WPC
were measured under different moisture
contents and relative humidities. It showed that
dielectric constant of wood increased
significantly with moisture content but no
significant difference was observed in the case
of WPC within the range of moisture contents
studied (Khan et al., 1991).
I. INTRODUCTION
Bamboo is a natural material. It has been
used traditionally as an engineering-structural
material for fabrication of village houses in all
stages of human culture development. In order
to utilize bamboo effectively under modern
scientific and technological conditions it is
necessary to study its properties. Bamboo is a
main material for bamboo-based panelsand a
wide range of bamboo products, including
bamboo articles for daily uses and bamboo
carbon (Zhang, 1995; Zhang et al., 2001).
Dielectric constant and dielectric loss
tangent is important factor of the dielectric
properties of bamboo. It has important
implications in the high-frequency and
microwave heating technology of bamboo
processing applications. Applications of
dielectric properties of bamboo and wood in
high-frequency and microwave heating
technology to determined drying, glueing,
softening and moisture content of bamboo and
wood (Yin, 1996).
Dielectric constant and tan d values of
different sections of bamboo cut from outer
skin to the central core have been determined
at different temperature range and frequency
range (Chand et al., 2006). It has been found
that dielectric constant and tan d increased with
increase of temperature and decreased with
from the center core to periphery outer surface
with increase of frequency.
The estimation of dielectric loss factor
which is considered a very important feature
for bamboo industry and wood industry,
properties of different wood species was done
by using soft computing algorithms as a
function of both ambient electro-thermal
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conditions applied during drying of wood and
basic wood chemistry (Iliadis et al., 2013).
Dielectric constant and dielectric loss
tangent of bamboo culm increased slowly with
the moisture content below fiber saturation
point (FSP), increased sharply with the
moisture content around the FSP, and when
above the FSP, it had a linear relation with the
moisture content. Dielectric constant of grain
direction was higher than that of other two
directions. It decreased obviously with the
increase of frequency, but changed slowly
when it above 6 kHz. Bamboo culm age,
different part of culm had no evident effect on
dielectric constant (Xu et al., 2012).
wood quite widely. However, very little work
has been done on the dielectric properties of
bamboo.
This study determined dielectric constant
and dielectric loss factor of bamboo at
different moisture contents and frequencies.
The main purpose is to provide the dielectric
properties of bamboo to determine the
parameters of high frequency press technology.
II. RESEARCH METHODOLOGY
2.1. Materials
The bamboo (Phyllostachys heterocycla cv.
pubescens) trees [6 years old, diameter ranging
from 7 to 12 cm] were collected from
Zhejiang, China. Approximately, the same
amount of bamboo semicircular fragments was
cut from the bamboo stem to prepare flat-
rolled. Bamboo samples were cut from these
bamboo strips with a diameter of 50 mm and
thickness of 5 mm. Uniformity of test sample
surfaces were polished by using a sanding
paper. Total of test samples were 12 samples.
2.2. Experimental methods
Bamboo or wood-like materials such as
WPC can be used as an important insulating
material for special applications. All untreated
woods had a higher dielectric constant than
their polymer composites. It is therefore
postulated that the presence of polymers has
led to a decrease in the number of polarizable
units (Chia et al., 1986).
2.1.2. Moisture adjustment
Dielectric properties of wood block treated
at various temperatures up to 800°C were
measured in the range from 20Hz to 1MHz and
from -150 - 20°C. These results suggested that
the electric conductivity decreased with
increasing temperature up to 400°C and a
small volume fraction of particles with large
conductivity is formed at microscopic levels in
the cell walls (Sugimoto et al., 2004).
Moisture adjustment was conducted in
drying cabinet. Based on experimental
requirements, all samples were put into drying
cabinet and the use of thermostat humidity
cabinet to adjust moisture content of bamboo
samples. All samples were conditioned for 0%
to 18% relative humidity to adjust. Moisture
adjustment times were 3 times, every time was
3
days. Moisture content adjustment
At present, study on dielectric properties of
parameters of bamboo samples in Table 1.
Table 1. Moisture content adjustment parameters of Bamboo
Adjustment parameters
Moisture
content
(%)
Time 1
Temperature (0C)
Time 2
Temperature (0C)
20
Humidity (%)
0 ÷ 2
Salt solution
0
6
-
1002
35
40
78
98
20
20
20
KNO3
NaCl
MgCl2
12
18
35
35
JOURNAL OF FORESTRY SCIENCE AND TECHNOLOGY NO. 5 - 2017
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The moisture content (MC) of the samples
were calculated according to the following
formula: MC (%) = [(m1-m0)/m0]×100, where
m1 is the weight of the sample before drying,
and m0 is the weight of the sample
immediately after drying.
2.1.2. Experimentalmethod
Figure 1 displays the flow chart when using
the 16451B for permittivity measurements.
Prepare the
dielectric material
Attach the guarded
electrode
Cable length
compensation
Connect the 16451B
Adjust the electrodes
Calculate permittivity
Compensate the
residual impedance
Set the measurement
conditions
Compensation
for adjustment
Insert the material
Cp-D measurement
Figure 1. Measurement procedure flow chart for the 16451B
When using an impedance-measuring
instrument to measure permittivity, the parallel
plate method is usually employed. An
overview of the parallel plate method is shown
in Figure 2.
capacitor. The measured capacitance is then
used to calculate permittivity. In an actual test
setup, two electrodes are configured with a test
fixture sandwiching dielectric material. The
impedance- measuring instrument would
measure vector components of capacitance (C)
and dissipation (D) and a software program
would calculate permittivity and loss tangent.
The parallel plate method, also called the
three terminal method in ASTM D150,
involves sandwiching a thin sheet of material
or liquid between two electrodes to form a
Figure 2. Parallel plate method
frequency range from 60 Hz to 6 MHz.
2.1.3. Measurement of Dielectric
The measurements of dielectric constant
(e’) and tan (d) values of bamboo samples
were made by using a Agilent 4294A Precision
Impedance Analyze with the 16451B, in the
moisture content range from 0% to 18% and
e’ was calculated by using the following
equations: e’ = (ta×Cp)/(A×e0), where Cp (F) is
equivalent parallel capacitance, ta (m) is
average thickness of test sample, A (m2) is area
of Guarded electrode, and e0 = 8.854×10-12
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[F/m]. Each sample had tested with 3 times.
Value of e’ and tan d were averaged.
bamboo sample increased in the order of the
treatment
moisture
contents
(0%<6%<12%<18%). Moisture content is the
dominating factor over duration of adjusting in
increasing e’. The same dielectric constant can
be obtained at lower treatment frequency with
lower moisture content or by using higher
treatment frequency with higher moisture
content. For example, with the same treatment
time were nine days, dielectric constant of
bamboo samples were about 6.0 0.5 when
moisture content at 6% for 60Hz but only
required 20% at 6 MHz.
III. RESULTS AND DISCUSSION
3.1. Dielectric constant (e’)
The change of dielectric constant as a
function of moisture content at several
frequencies for bamboo is shown in Figure 3.
It is visible that dielectric constant of bamboo
is directly related to treatment severity, which
depends on the moisture content. e’ increased
with increasing moisture content showing
anomaly at the transition MC from 0% to 18%.
e’ decreased with increasing frequency from
60 Hz to 6 MHz. e’ increased with increasing
severity of moisture content treatment. With
the same moisture content condition, in
general, e’ of treated bamboo sample decreased
in the order of the frequencies from small to
large. It is quite the reverse, with different
moisture content conditions on the same
bamboo sample, in general, e’ of treated
Dielectric constant of the bamboo in the dry
state has lowest value (2.0) and has highest
value 2.19 with different frequency.
Dielectric constant of the bamboo at MC
18% has the lowest value (6.68) with
frequency at 6 MHz and it has the highest
value (61.34) with frequency at 60 Hz.
70.00
60Hz
600Hz
6KHz
60KHz
600KHz
6MHz
60.00
50.00
40.00
30.00
20.00
10.00
-
0
2
4
6
8
10
12
14
16
18
20
Moisture content (%)
Figure 3. Variation of Dielectric constant e' for Bamboo at different moisture contents
and frequencies
Table 2 presents the two-way analysis of
variance (ANOVA) results of the e’ of
bamboo. Moisture content and frequency
showed significant effects on dielectric
constant, (P-value < 0.0001). In addition, these
two factors showed significant interaction on
the dielectric constant of bamboo.
JOURNAL OF FORESTRY SCIENCE AND TECHNOLOGY NO. 5 - 2017
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Table 2. Two-Factor Without Replication results of dielectric constant of bamboo
Source
f
MC
df
5
3
F-value
42.70
158.29
13.66
P-value
< 0.0001
< 0.0001
< 0.0001
f×MC
15
f – Frequency.
MC – Moisture content.
f×MC – Interaction of frequency and moisture content.
bamboo is near the fiber saturation point, the
movement speed of molecules bamboo is
faster, the electrical conductivity increased to
make dielectric constant increased. At lower
frequencies, because the water molecules's
dipolar are absorbed, lead to e’ values in the
bamboo is high.
This increase of e’ is due to the increased
mobility of water dipoles in bamboo. Water
has OH molecules and OH of water acts as a
dipole (Chand et al., 1994). These dipoles
contribute to the e’ behaviour of the bamboo.
The bound water content of bamboo gradually
increased when the moisture content of
bamboo increased, e’of water is relatively high
( 81) (Liu et al., 2004), lead to e’ increases
with increasing of water in bamboo. When
moisture content of bamboo is lower than the
fiber saturation point, the bound water of
bamboo fibers has not been in a saturated state.
Therefore, freedom degree of functional
groups in bamboo molecules are quite small,
kinetic energy of molecule is small that effect
the electrical conductivity, the dielectric
constant increases quite slowly. Dielectric
constant decreased when moisture content is
lower than 6% with frequency variation and
which increased quickly when moisture
content is larger than 12% with high frequency
3.2. Dielectric loss tangent d
The change of tan d value is shown in
Figure 4. It is visible that dielectric loss
tangent of bamboo was observed increasing
with increasing moisture constant and
decreasing with increasing frequency. Tan d
decreased when moisture content is lower than
6% and increased quickly when moisture
content is larger than 12%. Tan d increased
slowly with the moisture content below fiber
saturation point (FSP), increased sharply with
the moisture content around the FSP. Tan d
decreased sharply at the low frequency (< 6
KHz) and decreased slowly at the high
frequency (> 6 KHz).
value (> 6 KHz). The moisture content of
2.70
60Hz
600Hz
6KHz
6MHz
60KHz
600KHz
2.40
2.10
1.80
1.50
1.20
0.90
0.60
0.30
-
0
2
4
6
8
10
12
14
16
18
20
Moisture content (%)
Figure 4. Variation of Dielectric loss tangent d for Bamboo sample at different moisture contents
and frequencies
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Table 3 presents the two-way analysis of
variance (ANOVA) results of the tan d of
bamboo. Moisture content and frequency
showed significant effects on dielectric loss
tangent (P-value < 0.0001<). In addition, these
two factors showed significant interaction on
the dielectric loss tangent of bamboo.
Table 3. Two-Factor Without Replication results of dielectric loss tangent of bamboo
Source
f
df
5
F-value
14.85
37.60
5.69
P-value
< 0.0001
< 0.0001
< 0.0001
MC
3
f×MC
15
f – Frequency.
MC – Moisture content.
f×MC – Interaction of frequency and moisture content.
bamboo. Low moisture content (MC < 6%)
and high frequency variation (> 6 KHz) are
less effective on dielectric properties, but they
are very effective on dielectric properties a
thigh moisture content (MC > 12%) and low
frequency variation (<6 KHz). Dielectric
constant was small when the bamboo in the dry
state with different frequency value. Dielectric
constant of the bamboo at MC 18% was lowest
value (6.68) with frequency at 6 MHz and it
was highest value (61.34) with frequency at 60
Hz. Tan d decreased when moisture content is
lower than 6% and increased quickly when
moisture content is larger than 12%.
This decrease of tan d is mainly due to the
reduction of the hydroxyl group content in
bamboo. At lower frequency, a section of
water molecules and free radicals in molecular
organization of bamboo moved and actived
when the electric current changes, tan d
decreased sharply. Water molecules and free
radicals in molecular organization of bamboo
moving speed to late to keep up with changing
frequency, the number of actived free radicals
are reduced, conduction of electric current
inside bamboo decrease, tan d decreased
slowly. The lossy dielectric can be represented
by the circuit analog of a resistance in parallel
with a capacitor minimizes (Goodman et al.,
1991). At higher frequencies, the capacitor
offers low reactance minimizes the conduction
losses in the resistor. Hence, value of dielectric
loss decreases at the higher frequencies
(Vijendra Lingwal et al., 2003; Shiraneet al.,
1954). The tan d decrease from at all
frequencies.
(2) Dielectric constant (e’) and tan d
increased with the increase of moisture content
and decreased with the increase of frequency.
Dielectric constant (e’) and tan d increased
slowly with the moisture content below fiber
saturation point (FSP) and they increased
sharply with the moisture content around the
FSP.
(3) Dielectric constant (e’) and tan d
changed obviously when the frequency is
changing, and decreased with increasing
frequency. At lower frequency, tan d decreased
sharply. At higher frequency, tan d decreased
slowly. Dielectric constant and tan d decreased
obviously with the frequency below 6 KHz, but
they changed slowly when it is above 6 KHz.
IV. CONCLUSIONS
Dielectric properties that include dielectric
constant (e’) and dielectric loss tangent (tan d)
have been done in the moisture content range
from 0% to 18% and in the frequency range
from 60 Hz to 6 MHz. From the above results,
we can give some conclusions:
(1) Dielectric constant (e’) and tan d exist in
JOURNAL OF FORESTRY SCIENCE AND TECHNOLOGY NO. 5 - 2017
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32(6), 18-21.
8. Chia, L.H.L., Chua, P.H., Hon, Y.S., and Lee, E.
REFERENCES
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2. Zhang, Q.S., Jiang, S.X., and Tang, Y.Y. (2001).
Industrial utilization on bamboo (in Chinese).
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China Forestry Publishing House, Beijing.
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11. Liu, Y. X., and Zhao, G.J. (2004). Wood
Resource Materials Science. China Forestry Publishing
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Investigation on Gradient Dielectriec Characteristics of
Bamboo (Dentroclamusstrictus). J. App.Polym. Sci. 102,
380-386.
12. Goodman, G., Buchanan, R.C., and Reynolds,
T.G. (1991). In Ceramic Materials for electronics;
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6. Iliadis, L., Tachos, S., Avramidis, S., and
Mansfield (2013). Hybrid e-regression and validation
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(1954). Dielectric properties and phase transitions of
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ẢNH HƯỞNG CỦA ĐỘ ẨM VÀ TẦN SỐ ĐẾN ĐẶC TÍNH ĐIỆN MÔI
CỦA TRE (Phyllostachys heterocycla cv. pubescens)
Nguyễn Thị Hương Giang1, Trần Văn Chứ2
1,2 Trường Đại học Lâm nghiệp
TÓM TẮT
Độ ẩm của tre và giá trị tần số là những nhân tố quan trọng nhất ảnh hưởng đến đặc tính điện môi của tre. Đặc
tính điện môi lại là một trong những nhân tố quan trọng nhất dùng để xác định các thông số công nghệ của quá
trình ép nhiệt cao tần ván ghép khối tre. Vì vậy, việc nghiên cứu đặc tính điện môi của tre có ý nghĩa vô cùng
quan trọng... Trong bài viết này, độ ẩm của nguyên liệu tre được điều chỉnh từ 0 - 18% trong điều kiện phòng
thí nghiệm. Sau đó sử dụng thiết bị 4294A kết nối với máy phân tích trở kháng 16451B để xác định ảnh hưởng
của độ ẩm và tần số đến đặc tính điện môi của tre. Đặc tính điện môi bao gồm hằng số điện môi (e’) và góc tổn
thất điện môi (tan d) được xác định trong phạm vi độ ẩm từ 0 - 18% và tần số từ 60 Hz - 6 MHz. Kết quả
nghiên cứu cho thấy, hằng số điện môi (e’) và góc tổn thất điện môi (tan d) tăng khi độ ẩm của tre tăng và giảm
khi tần số tăng. Hằng số điện môi (e’) và góc tổn thất điện môi (tan d) tăng chậm khi độ ẩm dưới điểm bão hòa
thớ gỗ (FSP), tăng mạng khi độ ẩm tre gần với điểm bão hòa thớ gỗ FSP. Hằng số điện môi (e’) và góc tổn thất
điện môi (tan d) không tăng rõ ràng khi tần số ở dưới 6 KHz, nhưng lại thay đổi chậm khi tần số trên 6 KHz.
Từ khóa: Độ ẩm, góc tổn thất điện môi, hằng số điện môi, tần số, Tre.
Received
Revised
Accepted
: 05/8/2017
: 24/9/2017
: 05/10/2017
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